Search Advanced
2007 Volume 16 Issue 9
Article Contents
Previous Article Next Article

Lv Hui-Min, Chen Guang-De, Yan Guo-Jun, Ye Hong-Gang. 2007: Synthesis of hexagonal monocrystal AlN microtubes and nanowires at low temperature, Chinese Physics B, 16(9): 2814-2817.
Citation: Lv Hui-Min, Chen Guang-De, Yan Guo-Jun, Ye Hong-Gang. 2007: Synthesis of hexagonal monocrystal AlN microtubes and nanowires at low temperature, Chinese Physics B, 16(9): 2814-2817.
shu

Synthesis of hexagonal monocrystal AlN microtubes and nanowires at low temperature

  • Department of Applied Physics, Xi'an Jiaotong University, Xi'an 710049, China;Department of Applied Physics, Xi'an University of Technology, Xi'an 710048, China

  • Department of Applied Physics, Xi'an Jiaotong University, Xi'an 710049, China

  • Available Online: 30/09/2007
  • Fund Project: the National Natural Science Foundation of China(Grant 10474078)%the Science Foundation of the Education Office of Shanxi Province, China
  • This paper reports that pure hexagonal aluminium nitride microtubes and nanowires growing along the [0001] direction have been successfully synthesized by directly reacting AlCl3 with NaN3 at low temperature (450℃) under condition of non-solvent system. The grey-white powder of reacting product was characterized by high-resolution transmission electron microscope (HRTEM), which shows that the powder is long straight-wire morphology with outer diameter from 40 nm to 300 nm and length up to several micrometres. The results of both electron diffraction (ED)and x-ray diffraction (XRD) indicate that the AlN microtubes have a pure hexagonal monocrystal tubular structure with the combination of the curled AlN nanobelts. Room-temperature photoluminescence spectrum of the synthesized sample showed an emission peak, which is closely related to the small size of the microtubes.
  • 加载中
  • 加载中
通讯作者: 陈斌, bchen63@163.com
  • 1. 

    沈阳化工大学材料科学与工程学院 沈阳 110142

  1. 本站搜索
  2. 百度学术搜索
  3. 万方数据库搜索
  4. CNKI搜索
Export Citation
PDF
XML

Article Metrics

Article views(85) PDF downloads(0) Cited by(0)

Access History

Synthesis of hexagonal monocrystal AlN microtubes and nanowires at low temperature

  • Available Online: 30/09/2007

Abstract: This paper reports that pure hexagonal aluminium nitride microtubes and nanowires growing along the [0001] direction have been successfully synthesized by directly reacting AlCl3 with NaN3 at low temperature (450℃) under condition of non-solvent system. The grey-white powder of reacting product was characterized by high-resolution transmission electron microscope (HRTEM), which shows that the powder is long straight-wire morphology with outer diameter from 40 nm to 300 nm and length up to several micrometres. The results of both electron diffraction (ED)and x-ray diffraction (XRD) indicate that the AlN microtubes have a pure hexagonal monocrystal tubular structure with the combination of the curled AlN nanobelts. Room-temperature photoluminescence spectrum of the synthesized sample showed an emission peak, which is closely related to the small size of the microtubes.

    HTML

Reference (0)

Catalog

    /

    DownLoad:  Full-Size Img  PowerPoint
    Return
    Return